Here we report the synthesis at low temperature (220 °C) by a solvothermal method of highly crystalline LiCoPO4. This material is a candidate for application as cathode in next-generation Li-ion cells. The presented synthetic route allows a careful tailoring of the sample morphology and leads to morphologically homogeneous platelet-like particles. The obtained material has been characterized by synchrotron radiation X-ray diffraction, vibrational spectroscopies, X-ray photoemission spectroscopy and electron microscopies. The synthesized material has been also characterized in lithium cells to highlight its ability to reversibly cycle lithium.
Controlled synthesis of LiCoPO4 by a solvo-thermal method at 220 °c
S. Brutti;J. Manzi;A. De Bonis;F. Vitucci;A. Paolone;F. Trequattrini;
2015
Abstract
Here we report the synthesis at low temperature (220 °C) by a solvothermal method of highly crystalline LiCoPO4. This material is a candidate for application as cathode in next-generation Li-ion cells. The presented synthetic route allows a careful tailoring of the sample morphology and leads to morphologically homogeneous platelet-like particles. The obtained material has been characterized by synchrotron radiation X-ray diffraction, vibrational spectroscopies, X-ray photoemission spectroscopy and electron microscopies. The synthesized material has been also characterized in lithium cells to highlight its ability to reversibly cycle lithium.File | Dimensione | Formato | |
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