The microstructure and the oxidation resistance in air of continuous carbon fibre reinforced ZrB2-SiC ceramic composites were investigated. SiC content was varied between 5-20 vol.%, while maintaining fibre content at similar to 40 vol.%. Short term oxidation tests in air were carried out at 1500 and 1650 degrees C in a bottom-up loading furnace. The thickness, composition and microstructure of the resulting oxide scale were analysed by SEM-EDS and X-Ray diffraction. The results show that contents above 15 vol.% SiC ensure the formation of a homogeneous protective borosilicate glass that covers the entire sample and minimizes fibre burnout. The scale thickness is similar to 90 mu m for the sample containing 5 vol.% SiC and decreases with increasing SiC content.

Influence of SiC content on the oxidation of carbon fibre reinforced ZrB2/SiC composites at 1500 and 1650 degrees C in air

Vinci A;Zoli L;Sciti D
2018

Abstract

The microstructure and the oxidation resistance in air of continuous carbon fibre reinforced ZrB2-SiC ceramic composites were investigated. SiC content was varied between 5-20 vol.%, while maintaining fibre content at similar to 40 vol.%. Short term oxidation tests in air were carried out at 1500 and 1650 degrees C in a bottom-up loading furnace. The thickness, composition and microstructure of the resulting oxide scale were analysed by SEM-EDS and X-Ray diffraction. The results show that contents above 15 vol.% SiC ensure the formation of a homogeneous protective borosilicate glass that covers the entire sample and minimizes fibre burnout. The scale thickness is similar to 90 mu m for the sample containing 5 vol.% SiC and decreases with increasing SiC content.
2018
Istituto di Scienza, Tecnologia e Sostenibilità per lo Sviluppo dei Materiali Ceramici - ISSMC (ex ISTEC)
Ceramic-matrix composites (CMCs)
Ultra-High-Temperature-Ceramics (UHTCs)
Oxidation resistance
Microstructure
Carbon fibre
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Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/20.500.14243/342943
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