: Triply periodic minimal surface (TPMS) sandwich structures made from PLA, reinforced with flax fibers, offer a bio-based approach to lightweight design, but their performance is sensitive to material-extrusion parameters. This study investigates the combined effects of layer height (0.16, 0.24, and 0.28 mm) and extrusion temperature (200, 220 °C) on the flexural behavior of gyroid-core PLA-flax sandwiches. Six parameter combinations were fabricated by fused filament fabrication and tested in three-point bending to obtain flexural strength and strain at failure. Post-fracture optical microscopy related mesostructure and failure mechanisms to macroscopic response. The highest strength (≈23 MPa) was found at 0.28 mm/200 °C, while the greatest strain at failure (≈0.06 mm/mm) occurred at 0.16 mm/200 °C. Two-factor ANOVA showed the significant main and interaction effects of temperature and layer height on both metrics. Fractography revealed a transition from interfacial delamination at lower temperatures and thinner layers to a more localized, cohesive rupture as interlayer bonding improved with higher temperature and thicker layers. Complementary compression tests revealed a core-dominated cellular collapse, with first-collapse stresses ranging from 6.3 to 8.2 MPa and a significant dependence on layer height and temperature (ANOVA). A gate-to-gate sustainability assessment indicated that layer height dominates printing time, energy demand, and CO2 emissions, with 0.28 mm minimizing energy per unit property. Measured part masses were 4-6% below slicer predictions, consistent with typical FFF porosity. The results provide TPMS-specific process windows that balance mechanical performance and energy efficiency for PLA-flax sandwiches.

Influence of Layer Thickness and Extrusion Temperature on the Mechanical Behavior of PLA–Flax TPMS Sandwich Structures Fabricated via Fused Filament Fabrication

Chairi M.;Di Bella G.
2025

Abstract

: Triply periodic minimal surface (TPMS) sandwich structures made from PLA, reinforced with flax fibers, offer a bio-based approach to lightweight design, but their performance is sensitive to material-extrusion parameters. This study investigates the combined effects of layer height (0.16, 0.24, and 0.28 mm) and extrusion temperature (200, 220 °C) on the flexural behavior of gyroid-core PLA-flax sandwiches. Six parameter combinations were fabricated by fused filament fabrication and tested in three-point bending to obtain flexural strength and strain at failure. Post-fracture optical microscopy related mesostructure and failure mechanisms to macroscopic response. The highest strength (≈23 MPa) was found at 0.28 mm/200 °C, while the greatest strain at failure (≈0.06 mm/mm) occurred at 0.16 mm/200 °C. Two-factor ANOVA showed the significant main and interaction effects of temperature and layer height on both metrics. Fractography revealed a transition from interfacial delamination at lower temperatures and thinner layers to a more localized, cohesive rupture as interlayer bonding improved with higher temperature and thicker layers. Complementary compression tests revealed a core-dominated cellular collapse, with first-collapse stresses ranging from 6.3 to 8.2 MPa and a significant dependence on layer height and temperature (ANOVA). A gate-to-gate sustainability assessment indicated that layer height dominates printing time, energy demand, and CO2 emissions, with 0.28 mm minimizing energy per unit property. Measured part masses were 4-6% below slicer predictions, consistent with typical FFF porosity. The results provide TPMS-specific process windows that balance mechanical performance and energy efficiency for PLA-flax sandwiches.
2025
Istituto di Tecnologie Avanzate per l'Energia - ITAE
PLA–flax composites
additive manufacturing
bio-based materials
fused filament fabrication (FFF)
sandwich structures
sustainability
triply periodic minimal surface (TPMS)
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Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/20.500.14243/590646
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